I of Newton (The Twilight Zone)
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Sherman Hemsley is a professor whose day with the devil is nigh. Ron Glass, the devil proves he can do anything the professor can think up. When all is lost the professor comes through with one final act, of which the devil cannot overcome.
A bit of trivia: Watch the shirt Ron Glass is wearing if you ever get a chance to see this great episode. It changes what it says every time the camera shows what's written on it.